Experimental Setup and Models Validation
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چکیده
................................................................................................4.1 4.1 EXPERIMENTAL SETUP......................................................................4.2 4.2 AUTOMATED REACTORS...................................................................4.3 4.2.1 One Litre Reactor......................................................................................4.3 4.2.2 Five Litre Reactor .....................................................................................4.5 4.3 METHODS OF CHARACTERISATION.................................................4.7 4.3.1 Gravimetric Analysis ................................................................................4.7 4.3.2 Gel Permeation Chromatography ..............................................................4.8 4.3.3 Particle Size Distribution Analysis ..........................................................4.11 4.3.4 Nuclear Magnetic Resonance ..................................................................4.14 4.3.5 Differential Scanning Calorimetry...........................................................4.18 4.4 DYNAMIC MODEL VALIDATION .......................................................4.21 4.4.1 Monomer Conversion..............................................................................4.23 4.4.2 Particle Size Distribution and Average Diameter.....................................4.24 4.4.3 Molecular Weight Distribution and Averages..........................................4.26 4.4.4 Terpolymer Composition ........................................................................4.30 4.4.5 Glass Transition Temperature..................................................................4.31 4.5 MICROCALORIMETRY SOFT SENSOR VALIDATION .....................4.32 4.5.1 Polymerisation Rate ................................................................................4.34 4.5.2 Conversion..............................................................................................4.35 4.5.3 Polymer Composition..............................................................................4.38 4.6 CONCLUSION.....................................................................................4.40 BIBLIOGRAPHY .......................................................................................4.41 Chapter 4 Experimental Setup and Models Validation 4. 1 Experimental Setup and Models Validation
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